A status report and update of the instrumentation necessary to obtain spectra of molecules at high pressures are presented. The optical pressure cells used, the spectrophotometer needed to obtain the spectra, the optical link between the two, high pressure spectroscopic windows, pressure calibration methods, and future outlook of the technique will be determined. The use of the high pressure cells with the interferometric technique and for Raman spectroscopy is outlined.
FitchR. A.SlykhouseT. E., and DriekamerH. G., J. Opt. Soc. Am.47, 1015 (1957).
2.
FishmanE. and DriekamerH. G., Anal. Chem.28, 804 (1956).
3.
DrickamerH. G., “Optical Studies at High Pressure,” in Progress in Very High Pressure Research, BundyF. P.HibbardW. R. and StrongH. M., Eds. (Wiley, New York, 1961), p. 16.
4.
DrickamerH. G. and BalchanA. S., “High Pressure Optical and Electrical Measurements,” in Modern Very High Pressure Techniques, WentorfR. N., Ed. (Butterworth, London, 1962), p. 25.
5.
FerraroJ. R., “High Pressure Research in the Far Infrared Region,” in Far Infrared Properties of Solids, MitraS. S. and NudelmanS., Eds. (Plenum Press, New York, 1970), p. 451.
6.
FerraroJ. R., “High Pressure Vibrational Spectroscopy,” in Spectroscopy in Inorganic Chemistry, RaoC. N. R. and FerraroJ. R., Eds. (Academic Press, New York, 1971), p. 57.
7.
AdamsD. M. and PayneS. J., Ann. Rep. Progr. Chem. (A)69, 3 (1972).
8.
HamannS. D., “Effects of Intense Shock Waves,” in Advances in High Pressure Research, BradleyR. S., Ed. (Academic Press, New York, 1966), Vol. 1, p. 85; GreenE. F. and ToenniesJ. P., Chemical Reactions in Shock Waves (Arnold, London, 1964).
9.
LowndesR. P., Phys. Rev. B.1, 2754 (1970).
10.
BalchanA. S. and DrickamerH. G., Rev. Sci. Instr.31, 511 (1960).
11.
ShermanW. F., J. Sci. Instr.43, 462 (1966).
12.
RuncornS. K., J. Appl. Phys.27, 598 (1956).
13.
KlyuevY. A., Inst. Exp. Techn.5, 1 (1964).
14.
NoackK., Spec. Acta24A, 1917 (1968).
15.
PetersE. and ByerleyJ. J., Rev. Sci. Instr.34, 819 (1963).
16.
FishmanE. and DrickamerH. G., J. Chem. Phys.24, 548 (1956); FishmanE. and DrickamerH. G., Anal. Chem.28, 804 (1956).
17.
FangC. S.FoxJ. V.MaukC. E., and PrengleR. W., Appl. Spectrosc.24, 21 (1970).
18.
SchampH. W., Rev. Sci. Instr.30, 1051 (1959).
19.
GillS. J. and RummelW. D., Rev. Sci. Instr.32, 756 (1961).
20.
FerraroJ. R., Raman Newsletter, July, No. 55, 17 (1973).
21.
NicolM.EbisuzakiY.EllensonW. D., and KarimA., Rev. Sci. Instr.43, 1368 (1968).
22.
WeirC. E.LippincottE. R.Van ValkenburgA., and BuntingE. N., J. Res. Natl. Bur. Std. (U.S.) Sect. A.63, 55 (1959); LippincottE. R.WeirC. E.Van ValkenburgA., and BuntingE. N., Spec. Acta16, 58 (1960); LippincottE. R.WelshF. E., and WeirC. E., Anal. Chem.33, 137 (1961).
23.
BassettW. A.TakahashiT., and StookP. W., Rev. Sci. Instr.38, 37 (1967).
24.
FerraroJ. R. and QuattrochiA., Appl. Spectrosc.24, 102 (1971).
25.
AdamsD. M.PayneS. J., and MartinK., Appl. Spectrosc.27, 377 (1973).
26.
BarnettJ. D.BlockS., and PiermariniG. J., Rev. Sci. Instr.44, 1 (1973).
27.
FerraroJ. R. and TakemotoJ., Appl. Spectrosc.28, 66 (1974).
28.
(a) LippincottE. R. and DueckerH. C., Science144, 1119 (1964); (b) H. C. Duecker and E. R. Lippincott, Doctoral thesis, University of Maryland, College Park (1964).
29.
PostmusC.MaroniV. A., and FerraroJ. R., Inorg. Nucl. Chem. Letters4, 269 (1968).
30.
BraschJ. W. and LippincottE. R., Chem. Phys. Letters2, 99 (1968).
31.
MelvegerA. J.BraschJ. W., and LippincottE. R., Appl. Opt.9, 11 (1970).
32.
BraschJ. W. and JakobsenR. J., Spec. Acta21, 1183 (1965).
33.
BraschJ. W., J. Chem. Phys.43, 3473 (1965); JakobsenR. J.MikawaY., and BraschJ. W., Appl. Spectrosc.24, 333 (1970).
PostmusC.FerraroJ. R., and MitraS. S., Inorg. Nucl. Chem. Letters4, 155 (1968).
36.
McDevittN. T.WitkowskiR. E., and FateleyW. C., Abstract, 13th Colloquium Spectroscopium Internationale, June 18–24, 1967, Ottawa, Canada.
37.
BradleyC. C.GebbieH. A.KechinV. V., and KingJ. H., Nature211, 839 (1966).
38.
OwenN. B., J. Sci. Instr.43, 765 (1966).
39.
DanielsW. B. and HruschkaA. A., Rev. Sci. Instr.28, 1058 (1957).
40.
DanielsW. B., Rev. Sci. Instr.37, 1502 (1966).
41.
BrafmanO.MitraS. S.CrawfordR. K.DanielsW. B.PostmusC., and FerraroJ. R., Solid State Commun.7, 449 (1969).
42.
WalrafenG. E., “Structure of Water,” in Hydrogen-Bonded Solvent Systems, CovingtonA. K. and JonesP., Eds. (Taylor and Francis, London, 1968), p. 9.
43.
DavisA. B. and AdamsW. A., Spec. Acta27A, 2401 (1971).
44.
DaviesH. W., J. Res. Natl. Bur. Std. (U.S.)72A, 149 (1968).
45.
FerraroJ. R., Inorg. Nucl. Chem. Letters6, 823 (1970).
46.
FerraroJ. R.MeekD. W.SiwiecE. C., and QuattrochiA., J. Am. Chem. Soc.93, 3862 (1971).
47.
FormanR. A.PiermariniG. J.BarnettJ. D., and BlockS., Science176, 284 (1972); BarnettJ. D.BlockS., and PiermariniG. J., Rev. Sci. Instr.44, 1 (1973).
48.
AngellC. A. and AbkemeierM. L., Inorg. Chem.12, 1462 (1973).
49.
FoxJ. V. and PrengleH. W., Appl. Spectrosc.23, 157 (1969).
50.
DrickamerH. G. and ZahnerJ. C., “The Effect of Pressure on Electronic Structure,” in Advances in Chemical Physics, PrigogineI., Ed. (Interscience, New York, 1962), Vol. IV, p. 161; CarnallW. T.SiegelS.FerraroJ. R.TaniB., and GebertE., Inorg. Chem.12, 560 (1973).
51.
MargraveJ. L., “Matrix Isolation Spectroscopy,” in Spectroscopy in Inorganic Chemistry, RaoC. N. R. and FerraroJ. R., Eds. (Academic Press, New York, 1970), Vol. I, p. 57.
52.
BridgmanP. W., The Physics of High Pressure (G. Bell and Sons, London, 1952).
53.
BovenkerckH. P.BundyF. P.HallH. T.StrongH. M., and WentorfR. H., Nature184, 1094 (1959).
54.
BundyF. P.BovenkerckH. P.StrongH. M., and WentorfR. H., J. Chem. Phys.35, 383 (1961).
55.
WignerE. and HuntingtonH. B., J. Chem. Phys.3, 764 (1985).
56.
MetzW. D., Science180, 390 (1973).
57.
JayarananA.McWhanD. B.RemeikaJ. P., and DermierP. D., Phys. Rev. B.2, 3751 (1970).
58.
PistoriusC. W. F. T.PistoriusM. C.BlakeyJ. P., and AdmiraalL. J., J. Chem. Phys.38, 600 (1963).
59.
WhalleyE.HeathJ. B. R., and DavidsonD. W., J. Chem. Phys.48, 2362 (1967); WeirC. E. and Van ValkenburgA., J. Chem. Phys.32, 612 (1960).
60.
KellG. S. and WhalleyE., J. Chem. Phys.48, 2359 (1968).
61.
MitraS. S.PostmusC., and FerraroJ. R., Phys. Rev. Letters18, 455 (1967).
62.
PeercyP. S., Phys. Rev. Letters31, 379 (1973).
63.
PeercyP. S. and SamaraG. A., Phys. Rev. B.8, 2033 (1973).
64.
SamaraG. A. and PeercyP. S., Phys. Rev. B.7, 1131 (1973).
65.
DuranaS. C. and McTagueJ. P., Phys. Rev. Letters31, 990 (1973).
66.
CampbellJ. H. and JonasJ., Chem. Phys. Letters18, 441 (1973).
67.
MagyarG., Appl. Opt.13, 25 (1974).
68.
GeorgeP.BeetlestoneJ. G., and GriffithJ. S., Rev. Mod. Phys.36, 441 (1964).
69.
StrensR. G. J., “The Nature and Geophysical Importance of Spin Pairing in Minerals of Fe (II),” in The Application of Modem Physics to Earth and Planetary Interiors, RuncornS. K., Ed. (Wiley, London, 1969), p. 213.
70.
BurnsR. G., Minerological Applications of Crystal Field Theory (Cambridge University Press, Cambridge, 1970).
71.
BirchF., “Composition and State of the Earth's Interior,” in The Application of Modern Physics to the Earth and Planetary Interiors, RuncornS. K., Ed. (Wiley-Interscience, New York, 1969), p. 299.
72.
RingwoodA. E., Earth Planet. Sci. Letters2, 106, 255, 301 (1966).
73.
ReidA. F.WadsleyA. D., and RingwoodA. E., Acta Cryst.23, 736 (1967).